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产品推荐:6358-06-1(2-氯-5-氨基苯酚)

别名:2-氯-5-氨基苯酚
英文名称:2-Chloro-5-aminophenol
分子式:C6H6ClNO
Cas No.:6358-06-1
分子量:143.57
结构式:image.png

规格:98%

用途:基础原料、有机中间体、医药中间体

合成方法:

ethyl acetate; Pt/C

Reactants are commercially availlable.
Knight, Steven David, US2003/100580, A1, (2003) b). 2-Chloro-5-aminophenol A solution of 2-chloro-5-nitrophenol (25 g, 0.14 mol) in ethyl acetate (150 mL) was treated with 5percent Pt/C (250 mg) and the mixture shaken under a hydrogen atmosphere (30 psi) for 4 h. The mixture was filtered through Celiteg and the residue washed well with hot ethyl acetate. The filtrate was treated with activated charcoal and re-filtered as above. Evaporation of the ethyl acetate gave a solid (19.8 g, 98percent).